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无机及分析化学实验
目前,许多本科高校不断扩大本科留学生的招生规模,与国外高等院校开展中外合作办学并开设中外合作办学专业,同时部分高校理工科等专业也在尝试开设全英文化学专业类课程。无机及分析化学实验是一门独立的基础实验课程,是学生进入大学后的一门化学实验课程。它是研究元素及其化合物的性质、掌握定量分析方法以及基本操作和相关原理的一门化学实验课程,是培养学生化学实验技能与素质基础的实践环节。本教材是编者根据教学改革实践和教学发展需要,结合多年的教学讲义而编写的。内容包括:绪论、化学实验基本知识、化学实验基本操作、基础实验、提高性实验及设计实验。
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1 INTRODUCTION
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1.1 Laboratory Rules
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1.2 Laboratory Safety
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1.3 Laboratory Common Equipments
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1.4 Pre-lab Work
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1.5 Lab Reports
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1.6 Data Analysis
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2 EXPERIMENTS
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2.1 Calibration of Volumetric C-lassware
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2.2 Practice on Acid-base Titration
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2.3 Determination of Nitrogen Content in Ammonium Salt (Formaldehy de Method)
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2.4 Determination of the Hardness of Water
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2.5 Preparation and Calibration of Potassium Permanganate Solution
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2.6 Determination of Chloride in Water by Mohr Method
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2.7 Iodometric Titration of Vitamin C (Ascorbic Acid)
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2.8 Quantitative Determination of Sulfate by Gravimetric Analysis
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2.9 Determination of Dissociation Degree and Dissociation Constant of Acetic Acid
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2.10 Determination of of Catalyzed Decomposition Rate Constants of Hydrogen Peroxide
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2.11 Paper Chromatography Separation and Identification of Metal Cations
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2.12 Extraction of Spinach Pigments and Thin Layer Chromatography
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2.13 Purification on Raw Salt
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2.14 Some Properties on Alkali Metals and Halogens
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2.15 The Chemistry of Copper Group Elements and Quantitative Analysis by Titration
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2.16 The Chemistry of Nitrogen and Phosphorous
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2.17 Identification of Unknown Compounds
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2.18 Preparation and Quantitative Analysis of Sodium Thiosulfate
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2.19 Preparation and Composition Determination of Ferrous Oxalate
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2.20 The Preparation and Analysis of Calcium Iodate Ca(IO3)2
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2.21 Preparation and Zinc Content Determination of Zinc Gluconate
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2.22 Synthesis and Characterization of Geometrical Isomers of Dichlorobis (ethylenediamine)-Cobalt (I11) Chloride
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2.23 Synthesis and Characterization of The Complex his (N,N'-Disalicylalethylenediamine)-μ-Aquadicobalt (II)
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2.24 Spectrophotometric Determination of Iron
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2.25 Two-component Analysis of A Phenol/Benzoic Acid Mixture by UV-visible Spectroscopy
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2.26 Identification of Benzoic Acid and Aniline by Infrared Spectroscopy
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2.27 Determination of Calcium Content in Water Using Atomic Absorption Spectrometry
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2.28 Fluorescence Determination of The Content of Hydroxybenzoic Acid Isomers
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2.29 Matrix-Assisted Laser Desorption/Ionization (MALDI) Mass Spectrometry (MS) Analysis of Oligosaccharide
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2.30 Analysis Methods of Nuclear Magnetic Resonance (NMR) Spectroscopy
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2.31 Potentiometric Titration of Phosphoric Acid
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2.32 The Redox of Potassium Ferricyanide on Glassy Carbon Electrode
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2.33 Analysis of Alcohol in Alcoholic Beverages by Gas Chromatography
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2.34 The Separation and Quantification of Food Additives in Drinks Using High Performance Liquid Chromatography
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2.35 Thermal behavior and decomposition of copper sulfate pentahydrate
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3 Appendix
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3.1 Chemical Elements Listed by Atomic Mass
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3.2 Methods to Prepare Buffer Solutions
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3.3 Standard Electrode Potential
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3.4 Solubility Product Constant
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3.5 Organic Solvent Polarity
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- 4 References
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